What are potential errors in using a gas syringe?
What must be noted when recording gas volume?
What is the ideal gas equation?
PV = nRT
What is the molar gas volume at room temperature and pressure?
1 mol gas = 24 dm³
How can gas volumes be measured over water?
Using an up-turned measuring cylinder in a trough of water
What safety precautions should be taken with irritants?
Wear goggles
What should be done with corrosive substances?
Wear goggles
What is the first step in the detailed method for measuring gas?
Measure 30 cm³ of 1 mol dm⁻³ ethanoic acid
What is the final step of the gas measurement method?
Repeat the experiment increasing mass of calcium carbonate by 0.05 g each time
What is the purpose of using a gas syringe in experiments?
To measure the volume of gas and calculate moles or reaction rates
What is the formula to calculate moles from gas volume?
moles = PV/RT
What mass of calcium carbonate is used in the detailed method?
Approximately 0.05 g
How is the Mr of a volatile liquid calculated?
Mr = mass/moles
What is the calculated Mr of a volatile liquid if 0.150 g is injected?
53.4 g mol⁻¹
What is the volume of gas measured in the example provided?
80 cm³
What is the pressure in the example given?
100 kPa
What is the temperature in the example given?
70°C
What is the mass of CaCO3 used in the core practical?
0.25 g
How are moles of CO2 calculated from moles of CaCO3?
Assume moles of CO2 = moles of CaCO3
What is the formula for molar volume of CO2?
Molar volume of CO2 = volume of CO2 / moles of CO2
What happens to calcium sulphate crystals when heated?
CaSO4.xH2O(s) → CaSO4(s) + xH2O(g)
What is the first step in the method for heating calcium sulphate?
Weigh an empty clean dry crucible and lid.
What should be added to the crucible for the experiment?
Add 2g of hydrated calcium sulphate to the crucible.
Why should small amounts of solid (like 0.100 g) not be used?
Percentage uncertainties in weighing will be too high.
Why should large amounts (like 50g) of hydrated calcium sulphate not be used?
Decomposition is likely to be incomplete.
What is the purpose of the lid on the crucible during heating?
Prevents loss of solid but should be loose fitting to allow gas to escape.
What is the consequence of using a wet crucible?
It would cause mass loss to be too large due to water loss when heating.
What can the heating method be used for besides calcium sulphate?
Measuring mass loss in various thermal decomposition reactions.
What was the mass of hydrated zinc sulphate before heating?
3.51 g of hydrated zinc sulphate.
What was the mass of anhydrous zinc sulphate obtained?
1.97 g of anhydrous zinc sulphate.
How do you calculate the mass of H2O lost?
Mass of H2O = 3.51 g - 1.97 g = 1.54 g.
How do you calculate the moles of ZnSO4?
Moles of ZnSO4 = 1.97 / 161.5.
How do you calculate the moles of H2O?
Moles of H2O = 1.54 / 18.
What is the ratio of moles of ZnSO4 to H2O?
Ratio = 0.0122 / 0.085 = 1 / 7.
What is the value of x in ZnSO4.xH2O?
X = 7.
What is the first step in making a solution?
Weigh the sample bottle containing the required mass of solid on a 2 dp balance.
What should be done after adding distilled water to the beaker?
Stir to help dissolve the solid.
What should be done if the substance does not dissolve well in cold water?
Heat the beaker gently until all the solid has dissolved.
What is the purpose of rinsing the beaker and funnel?
To ensure all solid is transferred to the volumetric flask.
How should the volumetric flask be filled?
Fill so the bottom of the meniscus sits on the line on the neck of the flask.
What should not be done with a volumetric flask?
Do not heat or put hot solutions in the volumetric flask.
What is the advantage of using a volumetric pipette?
It is more accurate than a measuring cylinder due to smaller uncertainty.
What is the first step in diluting a solution?
Pipette 25cm3 of original solution into a 250cm3 volumetric flask.
What should be done after pipetting the original solution?
Make up to the mark with distilled water using a dropping pipette for last few drops.
What is the core practical for making a volumetric solution?
Carry out a simple acid–base titration.
What is the best method for measuring mass in experiments?
Measure mass on 2 or 3 d.p. balance of a weighing bottle.
What is a simple acid-base titration?
A quantitative chemical analysis method to determine the concentration of an acid or base by neutralizing it with a base or acid of known concentration.
What is the best method for measuring mass in experiments?
Measure mass on a 2 or 3 d.p. balance of a weighing bottle.
How many decimal places should the balance measure mass to?
2 or 3 decimal places (d.p.).
What are potential errors in using a gas syringe?
How can gas volumes be measured over water?
Using an up-turned measuring cylinder in a trough of water
What is the first step in the detailed method for measuring gas?
Measure 30 cm³ of 1 mol dm⁻³ ethanoic acid
What is the final step of the gas measurement method?
Repeat the experiment increasing mass of calcium carbonate by 0.05 g each time
What is the purpose of using a gas syringe in experiments?
To measure the volume of gas and calculate moles or reaction rates
What is the first step in the method for heating calcium sulphate?
Weigh an empty clean dry crucible and lid.
What should be added to the crucible for the experiment?
Add 2g of hydrated calcium sulphate to the crucible.
Why should small amounts of solid (like 0.100 g) not be used?
Percentage uncertainties in weighing will be too high.
Why should large amounts (like 50g) of hydrated calcium sulphate not be used?
Decomposition is likely to be incomplete.
What is the purpose of the lid on the crucible during heating?
Prevents loss of solid but should be loose fitting to allow gas to escape.
What is the consequence of using a wet crucible?
It would cause mass loss to be too large due to water loss when heating.
What can the heating method be used for besides calcium sulphate?
Measuring mass loss in various thermal decomposition reactions.
What is the first step in making a solution?
Weigh the sample bottle containing the required mass of solid on a 2 dp balance.
What should be done if the substance does not dissolve well in cold water?
Heat the beaker gently until all the solid has dissolved.
What is the purpose of rinsing the beaker and funnel?
To ensure all solid is transferred to the volumetric flask.
How should the volumetric flask be filled?
Fill so the bottom of the meniscus sits on the line on the neck of the flask.
What should not be done with a volumetric flask?
Do not heat or put hot solutions in the volumetric flask.
What is the advantage of using a volumetric pipette?
It is more accurate than a measuring cylinder due to smaller uncertainty.
What is the first step in diluting a solution?
Pipette 25cm3 of original solution into a 250cm3 volumetric flask.
What should be done after pipetting the original solution?
Make up to the mark with distilled water using a dropping pipette for last few drops.
What is the core practical for making a volumetric solution?
Carry out a simple acid–base titration.
What is the best method for measuring mass in experiments?
Measure mass on 2 or 3 d.p. balance of a weighing bottle.
What is a simple acid-base titration?
A quantitative chemical analysis method to determine the concentration of an acid or base by neutralizing it with a base or acid of known concentration.
What is the best method for measuring mass in experiments?
Measure mass on a 2 or 3 d.p. balance of a weighing bottle.
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